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[0041] The solvent used in the recrystallization of step 3) is chosen from Et 2 O, CH 2 Cl 2 , CHCl 3 , MeOH, CH 3 CN, THF, EtOAc, EtOH, Toluene, Hexane, Acetone or a mixed solvent of any thereof, preferably a mixed solvent of MeOH and CH 2 Cl 2