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Manual validation ensured accurate identification of all amino acid residues and post-translational modifications. Nuclear Magnetic Resonance (NMR) Spectroscopy To complement mass spectrometric data, ^1H and ^13C NMR spectroscopy were performed, providing insights into the conformational aspects and confirming the presence of specific functional groups, particularly in modified regions. Quality Control and Batch-to-Batch Comparability Assessment (New Section) Beyond single-batch characterization, peptide sequencing plays a vital role in establishing batch-to-batch consistency during late-stage development

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[PMID: 17113207 DOI: 10.1016/j.pnpbp.2006.10.001] [DOI] [PubMed] [Google Scholar] 70.Berk M, Copolov DL, Dean O, Lu K, Jeavons S, Schapkaitz I, Anderson-Hunt M, Bush AI

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Researchers managing multiple reconstituted vials need organized storage and clear labeling

Williams LM (2012) Hypothalamic dysfunction in obesity