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doi: 10.1517/14728222.2015.1025051 69 Lancet (1998)

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[0060] When condensing -Glu, use a reaction system in which the molar ratio of 2-chlorotriphenyl chloride resin / Fmoc-Glu(OH)-OtBu / HATU / DIPEA is 1:2:2:2.4, and react for 1.5h to obtain Fmoc- -Glu-AEEA-AEEA-resin, use 20% piperidine / DMF to deprotect after synthesis, the deprotection time is: 5+15min

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