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Reimann F, Habib AM, Tolhurst G, Parker HE, Rogers GJ, and Gribble FM
Fmoc deprotection was achieved with 20% piperidine in DMF (twice for 2 min, room temperature, 300 rpm shaking) and peptide couplings were performed as double or triple couplings (twice for 5 min, 75 C, 300 rpm shaking, except for Arg and His, for which twice for 5 min, 50 C, 300 rpm shaking) consisting of AA/HCTU/DIPEA (ratio, 1:1.25:2.5) in fivefold excess compared to the resin
doi: 10.1016/j.redox.2017.04.019
Gs/Gq signaling switch in cells defines incretin effectiveness in diabetes
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Filed in 1992 and granted in 1997, these patents only listed Habener
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