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Supercritical CO 2 was used as mobile phase A, while mobile phase B consisted of MeOH with 30 mM ammonium acetate and 2 % of H 2 O as the modifier, with MeOH with 0.1 % formic acid and 5 % water as the make-up solvent

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They both have a boxed warning on their drug labels that indicates a potential risk for thyroid tumors