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After experimentally determining TMT channel signal intensities, frozen samples were thawed, and a volume corresponding to 12.5 g/sample was combined in a new LoBind Eppendorf tube and dried using a SpeedVac

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doi:10.1007/s00210-023-02452-2

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The mixture was centrifuged at 40,000 RPM for 18 hr in a Beckman SW50.1 rotor at 21C

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