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The extract was rotary evaporated at 30 C to a volume of 2 ml, acidified to pH 4 with formic acid, and 200 l aliquots were purified using preparative HPLC (Agilent Technologies, 1260 Infinity) over a Luna 5 m phenyl-hexyl 100 (250 10 mm) column and a 15 min linear gradient from 0% acetonitrile in H 2 O to 16% acetonitrile in H 2 O at 4 ml min 1 flow

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Revised: May 2025 PRINCIPAL DISPLAY PANEL - 1.5 mL Pen Carton NDC 0024-5869-03 Rx only Toujeo SoloStar (insulin glargine) injection For Single Patient Use Only 300 units/mL (U-300) For subcutaneous use only Solution for injection in a disposable insulin delivery device Do not remove insulin with syringe Always use a new needle Do not mix with other insulins Use only if solution is clear and colorless with no particles visible Use within 56 days after opening *Needles not included (see back panel) Three 1.5 mL prefilled pens Dispense in this sealed carton sanofi PRINCIPAL DISPLAY PANEL - 3 mL Pen Carton NDC 0024-5871-02 Rx only Toujeo Max SoloStar (insulin glargine) injection For Single Patient Use Only 300 units/mL (U-300) Adjusts by 2 units For subcutaneous use only Solution for injection in a disposable insulin delivery device Do not remove insulin with syringe Always use a new needle Do not mix with other insulins Use only if solution is clear and colorless with no particles visible Use within 56 days after opening *Needles not included (see back panel) Two 3 mL prefilled pens Dispense in this sealed carton sanofi Biological Products Related to Toujeo SoloStar Find detailed information on biosimilars for this medication

A strong dose-response relation between serum concentrations of persistent organic pollutants and diabetes: results from the National Health and Examination Survey 1999-2002

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however, the precise role attributed to acetate in this regard still remains to be clarified